TOCOR700仪器使用手册.pdf

OPERATING INSTRUCTIONSTitleTOCOR700 UV(Ex)TOCOR700TOC Water AnalyzerInstallationOperationMaintenance2TOCOR700 Operating Instructions 8011462 V4.1 SICK AGDocument InformationDocument IDTitle:Operating Instructions TOCOR700Order No.:8011462Version:4.1Release:2013-01ProductProduct name:TOCOR700Variants:TOCOR700 UVTOCOR700 THTOCOR700 TH+2nd reactorSoftware:Version 1.10In these Operating Instructions,the designation TOCOR700 means that the information is applicable for all variants.ManufacturerSICK AGErwin-Sick-Str.1 79183 Waldkirch GermanyPhone:[phone]Fax:[phone]E-mail:info.pasick.dePlace of ManufactureSICK AGPoppenbtteler Bogen 9b 22399 Hamburg GermanyTrademarksNorprene and Tygon are trademarks of Saint-Gobain Performance Plastics Corporation.Viton is a trademark of DuPont Dow Elastomers.Swagelok is a trademark of the Swagelok Company.Other product names used in this Manual may also be trademarks and are only used for identification purposes.Guarantee InformationSpecified product characteristics and technical data do not serve as guarantee declarations.SICK AG.All rights reserved.GlossaryFIA:Flow Indication Alarm;measured value to monitor the carrier gas volume flowFirmware:Internal software of the device;mostly stored in eras-able storage modules(EEPROMs)LED:Light emitting diode(small display lights)NDIR:Non-dispersive infrared;designation for optical gas analysis methods in the infrared spectral rangePC:Personal ComputerTC:Total Organic Carbon(total carbon content)TIC:Total Inorganic Carbon(carbon content from inorganic sub-stances)TNB:Total Nitrogen Bound(total nitrogen content)TOC:Total Organic Carbon(carbon content from organic sub-stances)VAC:Volt Alternating Current(AC voltage)VDC:Volt Direct Current(DC voltage)TOCOR700 Operating Instructions 8011462 V4.1 SICK AG3Warning Symbols Warning levels/Signal wordsWARNINGRisk or hazardous situation which could result in severe personal injury or death.CAUTIONHazard which could result in less severe or minor injuries and/or material damage.NOTICEIndicates a hazard or unsafe practice which could result in property damage.Information SymbolsHazard(general)Hazard by voltageHazard in potentially explosive atmospheres Hazard by explosive substances/mixturesHazard by corrosive substancesHazard by poisonous substancesHazard by unhealthy substancesHazard by high temperature or hot surfacesHazard through ultraviolet radiation(UV light)Hazard for the environment/nature/organic life Information about the use in potentially explosive atmospheresImportant technical information for this deviceImportant information on electrical or electronic func-tionsSupplementary informationLink to information at another placeNice to knowContents4TOCOR700 Operating Instructions V4.1 8011462 SICK AG1Important Information.131.1Main hazards.141.2Important operating information.151.3Intended use .161.3.1Device function.161.3.2Installation location.161.3.3Intended users(target group).161.3.4Application limitations.171.4Responsibility of user.181.5Additional documents .192Product Description.212.1Product identification.222.2Know-how for the TOCOR700.232.2.1Measuring principle.232.2.2Measuring system.242.2.3Special advantages.252.3Device variants.262.3.1Reactor variants.262.3.2Individual device versions and documentation.262.3.3Versions for potentially explosive atmospheres.262.3.4Additional equipment.292.4Device design.302.4.1TOCOR700 UV(standard housing).302.4.2TOCOR700 TH(wall housing).322.5User Guide for the TOCOR700.342.5.1What must you do?.342.5.2What can you do in addition?.353Mounting and Assembly.373.1Delivery state.383.1.1Unpack and check.383.1.2Accessories and spare material included in scope of delivery.383.1.3Components packed separately(TOCOR700 TH).393.2Installation location.403.3Final device assembly.413.3.1Fill drain hoses(siphons)with water.413.3.2Fill the CO2 absorber.433.3.3Fill the corrosion inhibitor filter.443.3.4Fill the activated charcoal filter(only for TOCOR700 UV).453.3.5Fit the pump hoses.463.4Installing the reagent container.473.4.1Position and connect the reagent container.473.4.2Mixing the reagent.473.5Thermal reactor assembly(only for TOCOR700 TH).503.5.1Fill the reactor crucible.503.5.2Align the reactor crucible.523.5.3Assemble the thermal reactor.533.5.4Connect the thermal reactor.55ContentsContentsTOCOR700 Operating Instructions V4.1 8011462 SICK AG54Installation.574.1Housing installation .584.1.1Dimensions .584.1.2Mounting location,ambient conditions.584.2Waste water drain.594.3Gas outlet .594.4Liquid feed .604.4.1“Sample”connection.604.4.2“Single sample”connection.614.4.3“Zero solution”/“Test solution”connection.614.4.4“Reagent”connection.614.5External carrier gas feed.624.6Compressed air feed for the back-flush filter.624.7Purge gas feed for the pressurized enclosure .634.8Cable installation in potentially explosive atmospheres.634.9Mains connection.644.9.1Safety information for mains connection .644.9.2Connect the power cable .654.10Signal connections .664.10.1Position of signal connections.664.10.2Plug-in connectors of gas analyzer connection terminals.664.10.3Outputs for signal voltage(auxiliary voltage).674.11Safety information on signal connections.684.11.1Installation free of voltage.684.11.2Allowable load .684.11.3Signal voltages in potentially explosive atmospheres.684.11.4Suitable signal cables.694.11.5Protection against induced voltages .694.12Measured value outputs .704.13Analog inputs.714.14Switching outputs.724.14.1Switching functions .724.14.2Electrical function.724.14.3Connection contacts on the gas analyzer.734.15Control inputs.754.15.1Available control functions.754.15.2Electrical function.754.16Digital Interfaces.764.16.1Function of the interfaces.764.16.2Connecting the interfaces.765Start-up.775.1Main switch.785.2Start-up procedure .78Contents6TOCOR700 Operating Instructions V4.1 8011462 SICK AG6Operation(General).816.1LEDs on the gas analyzer.826.2Status messages on the display.836.3Principle of operation.836.3.1Function selection.836.3.2Display of menu functions(example).836.3.3Function keys.846.3.4Menu levels.856.4Selection switch for thermal reactors .867Standard Menu Functions.877.1Main menu .887.2Measuring displays.897.2.1Compact representation of measured values.897.2.2Large measured value display .907.2.3Chart recorder simulation .907.3Status displays .927.3.1Display status/fault messages.927.3.2Display measuring ranges.927.3.3Display measured value outputs .937.3.4Display alarm limit values .937.3.5Display instrument data.947.3.6Display drift values .957.4Control.967.4.1Switching the gas pump on/off.967.4.2Acknowledging alarms .977.4.3Setting the display contrast.987.4.4Setting the keypad click.987.4.5Switching reactor(s)on/off .997.4.6Switching the dosing pump on/off.997.4.7Switching the pre-sampling pump on/off(dosing pump M11).1007.4.8Switching single sample on/off .1007.4.9Switching dilution on/off(information).1007.5Calibration(information).1017.6Maintenance signal .1018Expert Menu Functions.1038.1Access to expert functions.1048.2Hidden expert functions .1048.3Local adaptation(localization).1058.3.1Language.1058.3.2Clock settings.1058.4Measured values display.1068.4.1Number of decimal places.1068.4.2Bargraph range.1068.5Influencing measured values.1078.5.1Damping(floating average computation).1078.5.2Dynamic damping .1088.5.3Measured value suppression at the start of the measuring range .109ContentsTOCOR700 Operating Instructions V4.1 8011462 SICK AG78.6Monitoring measured values .1108.6.1Alarm limit values.1108.6.2Overflow warnings.1118.7Configuration of calibrations(information).1118.8Configuration of measured value outputs .1128.8.1Special function with the“Sample point selector”option.1128.8.2Assigning measured value outputs.1128.8.3Configuring output ranges .1138.8.4Displaying of output ranges.1148.8.5Selecting output ranges .1148.8.6Setting live zero/deactivating a measured value output.1158.8.7Selecting the output mode during calibration.1158.8.8Deleting the settings for a measured value output .1168.9Configuration of switching outputs.1178.9.1Functional principle.1178.9.2Control logic.1178.9.3Safety criteria .1178.9.4Available switching functions(overview&explanation).1188.9.5Assigning switching functions.1198.10Configuration of status and control inputs .1208.10.1Functional principle.1208.10.2Available control functions(overview&explanation).1208.10.3Assigning control functions .1218.10.4Digital interface parameters .1228.10.5Automatic digital output of measured data.1238.10.6Printing configuration data(output as text table).1258.11Digital remote control(settings).1268.11.1Setting the ID character .1268.11.2Activating the ID character/activating Modbus.1278.11.3Setting the installed connection.1278.11.4Configuring the modem connection.1288.11.5Modem control .1298.12Data backup.1308.12.1Internal backup(saving the settings).1308.12.2External backup(data transmission).1318.13Firmware update.1348.14Volume flow adjustment and monitoring.1358.14.1Pump capacity(information).1358.14.2Flow limit value(information).1358.14.3FIA limit value .1368.14.4Carrier gas volume flow.1368.15TOCOR parameters.1378.15.1Back-flush filter settings(option).1378.15.2Dilution factor(information).1378.15.3Sample water limit value.1378.15.4Semi-continuous mode(information).137Contents8TOCOR700 Operating Instructions V4.1 8011462 SICK AG8.16Control functions of the gas analyzer.1388.16.1Measurement signals for measurement components.1388.16.2Status of internal controllers.1398.16.3Displaying internal analog signals.1398.16.4Internal supply voltages.1408.16.5Service display of internal analog signals .1408.16.6Linearization values.1418.16.7Status of control inputs .1418.16.8Program version.1418.17Sample point selector(option).1428.17.1Function of the sample point selector.1428.17.2Sample point selection results .1428.17.3Configuration of the sample point selector.1438.18Testing electronic outputs(hardware test).1448.19Reset.1459Calibration.1479.1Basic calibration information.1489.1.1Why is calibration necessary?.1489.1.2How does a calibration procedure in the TOCOR700 basically work?.1489.1.3Alternative calibration procedures.1499.1.4Alternative methods for zero point calibration.1499.1.5When is it necessary to perform a calibration?.1499.1.6Calibration liquid notation in the menus.1499.2Calibration liquids.1509.2.1Zero water.1509.2.2Calibration solution.1509.2.3Stock solution.1519.3Calibration preparation.1529.4Manual calibration.1539.4.1Manual calibration procedure.1539.5Automatic calibration.1569.5.1Requirements for automatic calibration(overview).1569.5.2Different automatic calibration routines.1569.5.3Setting-up an automatic calibration .1579.5.4Setting nominal values for calibration liquids.1589.5.5Setting drift limit values.1599.5.6Ignoring an external calibration signal.1609.5.7Setting a span delay time.1609.5.8Setting the calibration measuring time.1619.5.9Displaying automatic calibration settings .1629.5.10Starting the automatic calibration procedure manually.1639.6Displaying calibration data.1649.7Drift reset.1659.8Special calibrations .1669.8.1Basic settings for measuring sensitivity.1669.8.2Basic gas analyzer calibration .167ContentsTOCOR700 Operating Instructions V4.1 8011462 SICK AG910Remote Control with MARC2000.17110.1Introduction to remote control with MARC2000.17210.2Remote control installation.17310.2.1Electrical connection.17310.2.2Making the necessary settings in the TOCOR700.17610.2.3Setting the PC for remote control.17610.3Starting and ending remote control operation.17710.3.1Starting remote control.17710.3.2Status message during remote control with MARC2000 .17710.3.3Ending remote control.17810.4Remote control with“AK protocol”(information).17811Remote Control with Modbus.17911.1Introduction to the Modbus protocol.18011.2Modbus specifications for the TOCOR700.18111.3Installing a Modbus remote control.18211.3.1Interface.18211.3.2Electrical connection.18211.3.3Making the necessary settings on the TOCOR700.18211.4Modbus function commands for the TOCOR700.18311.4.1Function codes.18311.4.2Data formats.18411.4.3Modbus control commands.18511.4.4Modbus read commands .18612Maintenance.18912.1Scheduled maintenance .19012.1.1Maintenance plan .19012.1.2Maintenance protocol .19112.2Replacing expendable materials.19212.2.1Topping up reagent container.19212.2.2Replacing CO2 absorption material .19312.2.3Replacing the corrosion inhibitor filter.19512.2.4Replacing the activated charcoal filter .19612.2.5Replacing dosing pump hoses(5 channel hose pump).19712.2.6Replacing pre-sampling pump hoses(1 channel hose pump).19812.3Cleaning the UV reactor(TOCOR700 UV).19912.4Maintenance work on the thermal reactor(TOCOR700 TH).20112.4.1Safety information on the thermal reactor .20112.4.2Cleaning the reactor on a TOCOR700 TH(1 reactor).20212.4.3Cleaning the reactor on TOCOR700 TH+2nd reactor.20312.5Cleaning the waters lines.20412.6Preventive maintenance measures.20512.6.1Replacing the filter pads of the housing.20512.6.2Testing electrical signals.20512.6.3Care of the housing .20512.6.4Annual maintenance work by Customer Service.206Contents10TOCOR700 Operating Instructions V4.1 8011462 SICK AG13Troubleshooting.20713.1How the TOCOR700 signals a malfunction .20813.1.1Signs of a malfunction .20813.1.2Malfunction messages.20813.1.3Safety information on malfunction clearance .20813.1.4Support by Customer Service.20813.2General operational malfunctions.20913.2.1If the TOCOR700 does not function at all .20913.2.2When the reactor does not reach the nominal temperature.20913.3Malfunctions during measuring operation.21013.3.1When no measured values are displayed.21013.3.2When the measured value display is very unsteady .21013.3.3When measured values are obviously incorrect .21113.3.4If the reaction time(90%time)is too long .21213.4Malfunctions during calibrations.21213.4.1When zero point calibration is not possible .21213.4.2When sensitivity calibration is not possible .21213.5Leak tightness test.21313.6Status messages(in alphabetical order).21514Putting Out of Operation.22314.1Procedure to put out of operation.22414.2Short operating pauses.22514.3Disposal information.22515Storage,Transport.22715.1Correct storage.22815.2Transport over short distances.22915.3Correct shipping/transport over long distances .22916Custom Configuration Tables.23116.1Signal connections on gas analyzer(overview).23216.2User Table:Switching outputs Gas analyzer functions .23316.3User Table:Switching output TOCOR functions .23416.4User Table:Control inputs .235ContentsTOCOR700 Operating Instructions V4.1 8011462 SICK AG1117Spare Parts.23717.1UV reactor components(TOCOR700 UV).23817.1.1Spare parts .23817.1.2UV lamp service life.23917.1.3Replacing the UV lamp .23917.2Thermal reactor components(TOCOR700 TH).24017.3Pumps .24117.3.1Pump hoses for dosing pump(M10).24117.3.2Spare parts for the pre-sampling pump(dosing pump M11).24117.3.3Replacement pumps.24117.4Hoses.24217.5Glass contai